ASTM D(). Standard Guide for Testing Coating Powders and Powder Coatings. standard by ASTM International, 06/01/ View all product . Purchase your copy of ASTM D – 06() as a PDF download or hard copy directly from the official BSI Shop. All BSI British Standards. Mitsubishi GT06 Autotitrator. P-E Headspace .. Coating. Provider. From ASTM. D 5 Samples from powder coating lot to be used. 5.
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A number in parentheses indicates the year of last reapproval.
A superscript epsilon e indicates an editorial change since the last revision or reapproval. The test methods included are listed in Table 1. Where more than one test method is listed for the same characteristic, no attempt is made to indicate superiority of one method over another.
Selection of the methods to be followed must be governed by experience and the requirements in each individual case, together with agreement between the purchaser and the seller. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Current edition approved Feb. Originally published as D — Last previous edition D — Sampling Compatibility Lower explosion limit Particle size and distribution Multiple sieve and analysis Accelerated storage stability Glass vial method Pourability Fluidity Cured weight loss for thermosetting coating powders Gel time stroke cure Flow test incline method Speci?
Abrasion resistance Air blast abrasion tester Falling sand method Taber abraser Adhesion Tape adhesion Chemical resistance Household chemical resistance Detergent resistance Acid resistance Stains or reagents on wood substrates Chip resistance Gravelmeter Edge coverage Electrical insulation Elongation?
Color pigmented coatings Visual Instrumental For the reported hiding power to be signi? For thermoplastic materials, no chemical reaction takes place. Flow will re-occur if re-heated. Both thermoset and thermoplastic? It is applicable to both thermoplastic and thermoset coatings, unless indicated otherwise.
By design this guide does asm purport to address test methods or procedures developed speci? Information on current test procedures for pipe and reinforced steel bar d4351 powders and powder coatings can be obtained through their respective ASTM Subcommittees, A It should be noted that many of the methods used for characterizing a coating powder, such as gel time Section 16 and ast, Interpretation of the test results will depend on the speci?
These atm may be indicated by the individual test procedure used or agreed upon between the purchaser and seller. Problems such as changes in gloss, surface appearance, physical properties, and color contamination may occur if incompatible powders are mixed.
Rather than discover these problems on the production coating line, it is recommended that the compatibility of powders be checked prior to their use.
To obtain precise and reliable LEL results, it is best to employ the service of an independent laboratory, which has the special apparatus needed.
However, a quick calculation method, as listed below, has been proved in practice to be satisfactory when applied to coating application plants. Particle Size and Distribution There is unfortunately, no one optimum P. Accelerated Storage Stability In addition, the coating powder has to melt,? In the case of a thermoset coating powder, an accelerated storage stability test can allow a powder user to predict the physical and chemical stability of a coating powder in order to determine its long term usability as a function of time and temperature.
The physical stability of a thermoplastic coating powder can also be predicted.
ASTM D3451 – 06(2017)
Typically, the cured weight loss from a coating powder will consist of water and low molecular weight organic compounds or blocking agents, or both. The cured weight loss may be requested in order to properly determine the exhaust requirements of a bake oven or to comply with state or federal reporting guidelines. At this time, there is not a recognized ASTM standard test method for determining the cured weight loss for a coating powder; however, the following procedure has proven satisfactory in the?
The exact identity of the materials lost during the cure cycle would have to be determined by other means to identify what weight percent is organic and inorganic that is, water—see Note 1.
Refer to Practice D and local air quality regulations. By gentle tilting, spread the coating powder uniformly over the bottom of the dishes, then weigh to 0. NOTE 2—The recommended sample size of 0.
Flow Test Incline Method For a very smooth cured? On the other hand, if one needs to coat a part with sharp edges, a coating powder with relatively short? The chemistry of the coating powder can also in? This test is most useful to the coating powder formulator.
A coating powder is applied by volume mils thick by square feetbut often is purchased by weight pounds. Melting Point Determination NOTE 4—The impact fusion resistance of a coating powder is dependent on many factors, not just its melt temperature. Some coating powder chemistries can be inherently resistant to impact fusion even though their tack temperature might be relatively low. There may however, be speci? A deviation from the standard bake must be agreed upon between the purchaser and seller.
For test to test repeatability, it is recommended that the same oven be used for all cured weight loss testing. This test is 7 Allow 60 min for the warm up on the heating bar. Sprinkle a calibrating substance having the closest melting point to that of the powder on the heating bar. Observe the sharp division between solid and liquid.
Place the pointer between these two divisions. Observe the specimen after 1 to 2 min.
Brush the material towards the lower temperature and note the location where particles of powder adhere to the bar when brushed lightly. Place the x3451 at this point. Read the temperature and report in degrees Celsius.
Remove the powder quickly and thoroughly before the setting occurs. Do not use abrasives to clean the bar. There are many types of abrasion tests available and often one, more than the others, will best simulate the abrasion resistance required in a particular end use application.
Adhesion d341 can also be used for testing the degree of attachment between a primer powder coating or other coating type and a second coat of coating powder that is, intercoat adhesion.
Failure, when it occurs, is usually in the form of discoloration, changes in gloss, blistering, softening, swelling, or loss of adhesion. Field experience has shown that, in general, the higher the? It would therefore be bene? The following test method indicated has been found suitable for this purpose.
The results are most meaningful when a control powder, one whose? The comparison of results are only valid for coating powders tested in the same laboratory at about the same time, not results between different laboratories.
The type, application, and treatment of any undercoat system should be agreed upon between the ast, and the seller. It can also show whether there is any change in? Elongation is dependent on substrate type and? For powder coatings applied to coil strip or blanks, the standard elongation test used is the T-bend. The most widely recognized test for hardness is the pencil test. It should be noted however, that pencil hardness is not the most reproducible test and interpreting the results is somewhat subjective.
The results are highly dependent on such factors as; the pencil type used, the pressure exerted by the operator, and the care taken in preparing the pencil lead. Some industries that is, automotive have also adopted the use of Knoop Indention Hardness.
ASTM D – Standard Guide for Testing Coating Powders and Powder Coatings
There is no consistent correlation between the two tests. Impact resistance is dependent on the substrate type and its preparation, the thickness of the substrate, and the? Therefore, these test parameters should be agreed upon between the purchaser and the seller. Impact resistance has also been found to be a good indication of whether a coating powder has been adequately cured. They cover ashm of the pressure mottling and sticking, or blocking resistance of powder coatings applied to metal coil and blanks, or wood as they are stored prior to the?
The print test can determine the degree of marring due to pressure. Common terms associated with optical properties are de?
Key test methods or practices are as follows: In either case, it is important that the viewing and measurement conditions under which the color is to be evaluated are agreed upon between the purchaser and seller. If need be, color can also be visually evaluated using Practice Dwhich determines the Munsell Coordinates of the color of a coated surface.
A spectrophotometer, the preferred instrument, measures re? Spectrophotometers offer a choice of two standard observers, speci? Large area view is also recommended whenever possible. In either case, it is important that the viewing and s3451 conditions under which color difference is to be evaluated are agreed upon between the purchaser and seller see The color difference equation used should be agreed upon between purchaser and seller.
A mirror has a very high DOI, and a matte paint? The DOI of a paint? It asttm also important to know at what? In general, the lower the measuring angle, the greater the in? A powder coatings surface pro? Slight differences in the degree of orange peel are often difficult to quantify, and the evaluation can be somewhat subjective.